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Crystal Structure Analysis: A Primer (Iucr Texts on Crystallography), by Jenny Pickworth Glusker, Kenneth N. Trueblood
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This book aims to explain how and why the detailed three-dimensional architecture of molecules can be determined by an analysis of the diffraction patterns obtained when X rays or neutrons are scattered by the atoms in single crystals. Part 1 deals with the nature of the crystalline state, diffraction generally, and diffraction by crystals in particular, and, briefly, the experimental procedures that are used. Part II examines the problem of converting the experimentally obtained data into a model of the atomic arrangement that scattered these beams. Part III is concerned with the techniques for refining the approximate structure to the degree warranted by the experimental data. It also describes the many types of information that can be learned by modern crystal structure analysis. There is a glossary of terms used and several appendixes to which most of the mathematical details have been relegated.
- Sales Rank: #4104117 in Books
- Published on: 2010-08-23
- Original language: English
- Dimensions: 7.50" h x .80" w x 9.70" l, 1.84 pounds
- Binding: Hardcover
- 304 pages
Review
"This book would make an excellent text for an undergraduate and/or graduate level course in x-ray analysis of single crystals for structure determinations. It would also serve as a good introduction for an interested individual." --The Microscope
"Can be highly recommended as an undergraduate text...and... to any scientist who desires an introduction to structure determination....In producing their second edition, the authors have made the book even better by updating and judiciously enlarging it" --Acta Crystallographica
"This book is a truly excellent introduction to the concepts and practices of single-crystal diffraction. It is written in a comfortable style , and the illustrations...are generally excellent....I enthusiastically recommend it to beginning students." --Journal of the American Chemical Society
"An excellent book for people starting to learn to solve structures of crystals."--I. Kahn, Illinois Institute of Technology
About the Author
Jenny Pickworth Glusker took her doctorate at Oxford, before moving to the US for postdoctoral work at the California Institute of Technology in 1955. She is now Senior Member Emeritus at the Institute for Cancer Research, Fox Chase Cancer Center, Philadelphia, PA, and Adjunct Professor of Biochemistry and Biophysics, University of Pennsylvania, Philadelphia, PA. She has held various senior positions, including President of the American Crystallographic Association (1979), Chair of the U.S. National Committee for Crystallography (1982-1984), and visiting professorships at several universities worldwide. Awards include the Garvan Medal, American Chemical Society (1979), the Public Service Award, American Crystallographic Association (1991) and the Fankuchen Award, American Crystallographic Association (with Ken Trueblood, 1995).
Kenneth N. Trueblood took his Ph.D. in chemistry at the California Institute of Chemistry in 1947. He remained at the University of California, Los Angeles until his death in 1998. For his profound influence on beginning chemistry students, he received the first UCLA Distinguished Teaching award (1961) and the national award for excellence in teaching given by the Manufacturing Chemists Association in 1978. For his work he received a Fulbright award (1956-1957), a Guggenheim fellowship (1976-1977), and the Fankuchen Memorial award of the American Crystallographic Assn (1995). He was elected President of the American Crystallographic Association in 1961.
Most helpful customer reviews
10 of 10 people found the following review helpful.
The best introductory textbook on crystallography. Period
By Dr. Peter Muller
This is the third edition of a real classic! Ever since it first came out in 1971 the Glusker/Trueblood has been one of the best introductory texts on crystallography. It was updated the first time in 1985: Crystal Structure Analysis -- A Primer, second edition, however in the last 25 years crystallography has changed enough to make the second edition seem outdated. Therefore I sometimes preferred the also excellent book by Massa Crystal Structure Determination, which does not cover quite as much ground but was more up-to-date. The "better" is the strongest enemy of the "good" and with the advent of the third edition of the Glusker/Trueblood, I am now recommending "Crystal Structure Analysis: A Primer" by Jenny Glusker and Ken Trueblood without hesitation to anyone who wants to learn more about crystallography. Every aspect from definition of a crystal to the diffraction experiment, phase problem, symmetry in real and reciprocal space, structure refinement and critical interpretation of the results is covered by this fabulous book and every chapter is perfectly up-to-date (even taking into consideration research conducted in 2009).
I would like to point out a few highlights:
(1) The chapter on Direct Methods absolutely stellar. It is better than any attempt to tackle this difficult topic I have ever seen. Even if you are already fairly advanced in crystallography but haven't quite understood how Direct Methods work: chapter 8 of this book will help you.
(2) Unlike many other textbooks the Glusker/Trueblood is very critical with the method it introduces. Crystal structure determination is sometimes seen by the uninformed as a sort of magic method that creates perfect pictures of molecules out of thin air. The Gluserk/Trueblood describes potential pitfalls and it makes very clear what you can and what you can not learn from a crystal structure. This is important information especially for beginners and "casual users" of crystallography.
(3) Throughout all chapters, the book contains numerous historical references to early scientists and key experiments, some dating back well over hundred years. This may not be vital for understanding modern crystallography, but learning about the history puts everything into perspective.
Further reading:
Another excellent beginner's text on crystallography is the above mentioned book by Werner Massa: Crystal Structure Determination.
A good book to deepen the knowledge one has gained from a beginner's book like the Glusker/Trueblood is Fundamentals of Crystallography by Carmelo Giacovazzo.
If you want to take it one step further and are getting into the refinement of crystal structures, I can recommend Crystal Structure Refinement: A Crystallographer's Guide to SHELXL.
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